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HERBAL ANTI-OXIDANT MOISTURIZING FORMULATION

ORDINARY APPLICATION

Published

date

Filed on 15 November 2024

Abstract

The present invention is related to the 5 herbal anti-oxidant moisturizing formulation comprising of non-comedogenic cold compressed oils like jojoba oil, grapeseed oil, rosehip oil, argan oil in the presence of pharmaceutically acceptable excipients. The said formulation is non-comedogenic and vegan cream-based moisturizer that offers a natural and potent remedy for various skin concerns, including hydration, 10 anti-aging, and protection against environmental damage, without clogging pores or using animal-derived ingredients. .

Patent Information

Application ID202421088467
Invention FieldBIOTECHNOLOGY
Date of Application15/11/2024
Publication Number49/2024

Inventors

NameAddressCountryNationality
Smita Datta KadamCelestial Phase I, I 801, Ravet Pune, 412101 Maharashtra, IndiaIndiaIndia

Applicants

NameAddressCountryNationality
Smita Datta KadamCelestial Phase I, I 801, Ravet Pune, 412101 Maharashtra, IndiaIndiaIndia

Specification

Description:FIELD OF THE INVENTION
[001] The present disclosure in general pertains to the field of herbal anti-oxidant
moisturizing formulations. In pa 5 rticular, the present disclosure relates to the herbal
anti-oxidant moisturizing formulation comprising of non-comedogenic cold
compressed oils like jojoba oil, grapeseed oil, rosehip oil, argan oil in the presence
of pharmaceutically acceptable excipients. More particularly, the present disclosure
relates to the vegan herbal anti-oxidant moisturizing formulation comprising of
10 non-comedogenic cold pressed oils in the form of cream for addressing various skin
concerns, including hydration, anti-aging, and protection against environmental
damage, without clogging pores or using animal-derived ingredients.
BACKGROUND OF THE INVENTION
15 [002] The skin, being the largest organ of the human body, serves as the first line
of defence against environmental stressors, including UV radiation, pollution, and
various toxins. These external factors can lead to the generation of free radicals,
which are highly reactive molecules capable of damaging cellular components such
as lipids, proteins, and DNA. This oxidative stress accelerates skin aging,
20 characterized by the appearance of wrinkles, fine lines, and loss of elasticity.
[003] Antioxidants, which neutralize free radicals, have emerged as essential
ingredients in skincare formulations aimed at preventing or reducing the damage
caused by oxidative stress. When incorporated into moisturizers, antioxidants not
only provide hydration but also offer a protective barrier against environmental
25 aggressors. A well-formulated antioxidant moisturizer can therefore play a crucial
role in maintaining skin health, improving its texture, and delaying the visible signs
of aging.
[004] The formulation of an antioxidant moisturizer requires a careful selection of
ingredients that are stable, effective, and compatible with the skin. Common
30 antioxidants used in skincare include vitamin C, vitamin E, coenzyme Q10, and
3
plant-derived polyphenols, each offering unique benefits. There are several skin
types, including normal skin which is balanced in terms of moisture, oil, and
sensitivity, normal skin tends to be smooth with few imperfections; Oily Skin
characterized by excess sebum production, oily skin often has enlarged pores and
is prone to acne and blackheads; Dry Skin lacking 5 in natural oils, dry skin can feel
tight, rough, and may be prone to flaking and irritation and sensitive skin that is
easily irritated, sensitive skin may react to certain products or environmental
factors, leading to redness, itching, or burning.
[005] Currently there are many herbal anti-oxidant moisturizing formulations
10 available in the market. One such product available is sold under the brand "Cuccio
GRAPESEED Anti-Oxidant Oil with Jojoba, Sunflower Seed Oil" used for
Smoothing Moisture & Repair Dry Cracked Skin, Firming Oil, and Reduce Fine
Lines & Signs of Aging. But the said product being the facial oil, typically lacks
the variety of ingredients found in cream formulations, such as humectants and
15 emollients that provide comprehensive skincare benefits. Further the facial oils can
leave a greasy residue on the skin, which may be uncomfortable for people with
oily or acne-prone skin.
[006] Other herbal anti-oxidant moisturizing products available in the market
include "Ayuveer Gold Facial Cream with Saffron, Jojoba & Argan Oil" and
20 "Zobha Facelift Moisturizer Lotion with Grape Seed Oil & Safflower". However,
these products contain synthetic and comedogenic ingredients that can cause
irritation and clog pores. Further Ingredients like Cyclopentasiloxane can
accumulate on the skin or hair, leading to clogged pores and environmental
concerns.
25 [007] Hence, there is need for natural and non-comedogenic products that
effectively hydrate, protect, and rejuvenate the skin without causing pore blockage
or irritation.
4
[008] Accordingly, the present invention by addressing the drawbacks in the prior
art, has developed Vegan herbal anti-oxidant moisturizing formulation comprising
of non-comedogenic oils, butters and natural extracts along with pharmaceutically
acceptable excipients that provides a wider range of skincare benefits without
causing pore blockage or irritation. The said 5 formulation has a lighter, non-greasy
texture, making it more suitable for daily use and less likely to leave a greasy
residue.
SUMMARY OF THE INVENTION
10 [009] The present invention is related to the herbal anti-oxidant moisturizing
formulation comprising of non-comedogenic oils and pharmaceutically acceptable
excipients along with the preparation method thereof.
[0010] In one aspect of the present invention, disclosed herein is the herbal anti15
oxidant moisturizing formulation comprising of non-comedogenic oils like jojoba
oil, grapeseed oil, rosehip oil, argan oil, shea butter, carrot seed extract, papaya
liquid extract and licorice liquid extract in the presence of pharmaceutically
acceptable excipients selected from emollients, humectants etc.
20 [0011] In another aspect of the present invention, the said herbal anti-oxidant
moisturizing formulation is a cream-based vegan formulation.
[0012] In yet another aspect of the present invention, during physiochemical
evaluation, the pH of the said formulation ranges between 5.5 to7 and the viscosity
25 ranges between 20000 - 100000 cps. The dermatology report during laboratory
testing of the said herbal anti-oxidant moisturizing cream indicates 0 score for
comedogenic rating with no irritation thereby confirming that the said cream depicts
no comedones or skin irritation. Further, microbial analysis during laboratory
testing confirms the anti-microbial activity and thermal stability.
5
[0013] In yet another aspect of the present invention, the said herbal anti-oxidant
moisturizing formulation hydrates, protects, and rejuvenates the skin with no
clogged pores and irritation. It offers a safe and effective way to nourish the skin
without clogging pores, while also aligning with the growing demand for
sustainable, c 5 ruelty-free beauty products.
DETAILED DESCRIPTION OF THE INVENTION
[0014] The following is a detailed description of embodiments of the present
disclosure. The embodiments are in such detail as to clearly communicate the
disclosure. However, the amount of detail offered is not intended to limit the
10 anticipated variations of embodiments; on the contrary, the intention is to cover all
modifications, equivalents, and alternatives falling within the spirit and scope of the
present disclosure as defined by the appended claims.
[0015] Unless the context requires otherwise, throughout the specification which
follow, the word "comprise" and variations thereof, such as, "comprises" and
15 "comprising" are to be construed in an open, inclusive sense that is as "including,
but not limited to."
[0016] Reference throughout this specification to "one embodiment" or "an
embodiment" means that a particular feature, structure or characteristic described
in connection with the embodiment is included in at least one embodiment. Thus,
20 the appearances of the phrases "in one embodiment" or "in an embodiment" in
various places throughout this specification are not necessarily all referring to the
same embodiment. Furthermore, the particular features, structures, or
characteristics may be combined in any suitable manner in one or more
embodiments.
25 [0017] The headings and abstract of the invention provided herein are for
convenience only and do not interpret the scope or meaning of the embodiments.
6
[0018] The present disclosure discloses the herbal anti-oxidant moisturizing
formulation comprising of non-comedogenic cold compressed oils like jojoba oil,
grapeseed oil, rosehip oil, argan oil in the presence of pharmaceutically acceptable
excipients.
5
[0019] In the preferred embodiment of the present disclosure, the herbal antioxidant
moisturizing formulation comprising of; 4% each of cold compressed
Grapeseed oil, cold compressed Rosehip oil, cold compressed Jojoba oil and cold
compressed Argan oil; 0.5% each of Liquorice Liquid Extract, Papaya Liquid
10 Extract and Carrot seed Liquid Extract; 2% each of Candelilla wax, Shea butter and
Glycerin; 1% each of Geogard ECT, Vitamin E and Cherry blossom Flavour; 9%
Emulsifying wax; 0.02% Rose Pink Mica Powder and 64.48% (q.s. to make 100
gms) distilled water.
15 [0020] In an embodiment of the present disclosure, the said herbal antioxidant
moisturizing formulation has been formulated using non-comedogenic natural
ingredients like Grapeseed oil, Jojoba oil, Rosehip oil and Argan oil wherein the
said oils synergistically enhance moisturizing, hydrating and antioxidant properties
and ability to support skin health without causing comedogenicity.
20
[0021] In an embodiment of the present disclosure, Liquorice Liquid Extract,
Papaya Liquid Extract and Carrot seed Liquid Extract in the said the said herbal
antioxidant moisturizing formulation has antioxidant, anti-inflammatory, and
rejuvenating properties. These extracts further assist in reducing hyperpigmentation
25 and improving the overall appearance of the skin.
[0022] In another embodiment of the present disclosure, Candelilla wax, Shea
butter are used as emollients while Glycerin, emulsifying wax and Vitamin E are
used as humectants in the said herbal antioxidant moisturizing formulation.
7
[0023] In another embodiment of the present disclosure, Geogard ECT has been
used as a preservative in the said herbal antioxidant moisturizing formulation.
[0024] In another embodiment of the present disclosure, Rose Pink Mica Powder
has been used as softening and anti-ageing agent in the said herbal antioxidant
5 moisturizing formulation.
[0025] In another embodiment of the present disclosure, the said herbal antioxidant
moisturizing formulation is a Vegan cream-based formulation.
[0026] In another embodiment of the present disclosure, during physiochemical
evaluation, the pH of the said formulation ranges between 5.5 to7 with the preferred
10 pH of 6.5 and the viscosity ranges between 20000 - 100000 cps with the preferred
viscosity. The dermatology report during laboratory testing of the said herbal antioxidant
moisturizing cream indicates 0 score for comedogenic rating with no
irritation thereby confirming that the said cream depicts no comedones or skin
irritation. Further, microbial analysis during laboratory testing confirms the anti15
microbial activity and thermal stability.
[0027] In an exemplary embodiment of the present disclosure, a method of
preparation of the said herbal anti-oxidant moisturizing cream comprises of;
a. adding Grapeseed oil, Rosehip oil, Jojoba oil, Argan oil, emulsifying wax,
candelilla wax and Shea Butter in a prescribed quantity in a container and melting
20 the same in the water bath at maintained temperature of 70°-80°C under slow
stirring to form oil phase;
b. adding distilled water and glycerin in the prescribed quantity in another container
and heating the same in the water bath at maintained temperature of 70°-80°C under
slow stirring to form aqueous phase;
25 c. filtration of oil phase in step a. through sieve no. 100 and adding the same to
aqueous phase;
8
d. mixing and homogenizing the mixture prepared in step c. up to 30 mins until
formation of cream;
e. continue mixing until the cream base is cooled to 40°-45°C;
f. adding Geogard ECT, Vitamin E, Cherry blossom Flavour, Liquorice Liquid
Extract, Papaya Liquid Extract and Carrot seed 5 Liquid Extract along with Rose Pink
Mica Powder to the cream base in step g under slow stirring initially and continuous
stirring later with homogenization for 10 minutes.
[0028] In yet another embodiment of the present disclosure, the said herbal antioxidant
moisturizing cream is suitable for all types of skin including dry skin, oily
10 skin, sensitive and acne-prone skin.
[0029] In yet another embodiment of the present disclosure, the said herbal antioxidant
moisturizing cream has a lighter, non-greasy texture, making it more
suitable for daily use and less likely to leave a greasy residue.
[0030] In yet another embodiment of the present disclosure, the said herbal anti15
oxidant moisturizing cream is easier to apply evenly and absorbs more quickly,
making it suitable for use under makeup.
[0031] In yet another embodiment of the present disclosure, the said herbal antioxidant
moisturizing cream is non-comedogenic, free from harsh chemicals, and
includes naturally derived preservatives.
20 [0032] In yet another embodiment of the present disclosure, the said herbal antioxidant
moisturizing cream has been developed for face and skin care wherein the
said non-comedogenic and vegan moisturizer offers a natural and potent remedy for
various skin concerns, including hydration, anti-aging, and protection against
environmental damage, without clogging pores or using animal-derived
25 ingredients.
9
[0033] In another embodiment of the present disclosure, the said herbal anti-oxidant
moisturizing cream hydrates, protects, and rejuvenates the skin while minimizing
the risk of clogged pores and irritation.
Advantages of the Herbal anti-oxidant moisturizing cream
1. The said herbal anti-oxidant moisturizing cream 5 is vegan and the presence
of non-comedogenic oils offers a safe and effective way to nourish the skin
without clogging pores, while also aligning with the growing demand for
sustainable, cruelty-free beauty products.
2. The said herbal anti-oxidant moisturizing cream is gentle and safe for all
10 types of skin including acne prone skin.
3. The synergistic composition of the natural ingredients and extracts in the
said herbal anti-oxidant moisturizing cream promotes skin regeneration,
hydration and moisture retention.
4. The said herbal anti-oxidant moisturizing cream has soothing and calming
15 properties.
5. The said herbal anti-oxidant moisturizing cream promotes holistic wellbeing
6. The said herbal anti-oxidant moisturizing cream brightens and evens the
skin tone.
20 Other embodiments of the present disclosure will be apparent to those skilled in the
art from consideration of the specification and practice of the disclosed
embodiments. The following examples should be considered as exemplary only,
with a true scope and spirit of the present disclosure being indicated by the claims.
25
10
EXAMPLES:
Preparation of Herbal anti-oxidant moisturizing cream
Add 4% each of Grapeseed oil, Rosehip oil, Jojoba oil and Argan oil, 9% of
emulsifying wax, 2% each of candelilla wax and Shea Butter a container and melt
the same in the water 5 bath at maintained temperature of 70°-80°C under slow
stirring to form oil phase. Add sufficient quantity of distilled water to make the
quantity 100 gms and 2% of glycerin in another container and heat the same in the
water bath at maintained temperature of 70°-80°C under slow stirring to form
aqueous phase. Filter the oil phase through sieve no. 100 and add it to aqueous
10 phase. Mix and homogenize the mixture prepared up to 30 mins until formation of
cream. Mix the mixture continuously until the cream base is cooled to 40°-45°C.
Add 1% each of Geogard ECT, Vitamin E, Cherry blossom Flavour and 0.5% each
of Liquorice Liquid Extract, Papaya Liquid Extract and Carrot seed Liquid Extract
along with 0.02% of Rose Pink Mica Powder to the cream base with slow stirring
15 initially and continuous stirring later with homogenization for 10 minutes.
Table 1: Composition of Herbal anti-oxidant moisturizing cream
Ingredients % Qty. w/w Qty./100g.
Cold Compressed Grapeseed oil 4.00 4.00
Cold Compressed Rosehip oil 4.00 4.00
Cold Compressed Jojoba Oil 4.00 4.00
Cold Compressed Argan Oil 4.00 4.00
Emulsifying wax 9.00 9.00
Candelilla wax 2.00 2.00
Shea Butter 2.00 2.00
Glycerin 2.00 2.00
Liquorice Liquid Extract 0.5 0.5
Papaya Liquid Extract 0.5 0.5
Carrot seed liquid Extract 0.5 0.5
11
Evaluation of Herbal anti-oxidant moisturizing cream
Organoleptic Evaluation
Table 2: Organoleptic Evaluation of Herbal anti-oxidant moisturizing cream
5
Physicochemical Evaluations
pH evaluation:
10
pH of 1% aqueous solution of the formulation was measured by using a calibrated
digital PH meter at constant. the pH of the said herbal anti-oxidant moisturizing
cream is in the range of 5.5 - 7 with the preferred pH of 6.5 as indicated in Table 3
below.
15 Viscosity
The viscosity of the Moisturiser was determined by using Brookfield Viscometer
using the spindle no 93 and temperature of the product was maintained at 25°C as
indicated in Table 3 below. The viscosity of the said herbal anti-oxidant
moisturizing cream is in the range of 20000 - 100000 cps with the preferred
20 viscosity of 50,000 cp.
Table 3: Physiochemical Evaluation of Herbal anti-oxidant moisturizing cream
Geogard ECT, 1.00 1.00
Vitamin E 1.00 1.00
Cherry blossom Flavour 1.00 1.00
Rose Pink Mica Powder 0.02 0.02
Purified Water I.P. 64.48 q.s. to make
100.00 g
PARAMETER RESULTS
Colour Baby Pink
Odour blend of pink Japanese cherry blossoms and
fragrant mimosa flower petals, warm base notes
of vanilla, Tonka bean, and oriental woods
Texture Fine
Appearance soft, homogeneous cream
PARAMETER RESULTS
pH 6.5
12
Spreadability test
Procedure:
1 g of Moisturiser was placed on the centre of 5 a glass plate. AA second glass plate
was placed over the cream, and a 500 g weight was applied on top. The weight was
left on the sample for 5 minutes to allow the cream to spread. After 5 minutes, the
weight and top glass plate were removed. The diameter of the spread cream was
measured to be 8 cm.
10 Calculation:
Using the formula for spreadability:
Spreadability=m×l/t
Where:
m = 500 g (weight applied)
15 l = 8 cm (diameter of the spread cream)
t = 5 minutes (converted to seconds = 300 seconds)
Spreadability=500×8/300=13.33 g/cm/sec
Interpretation of Results:
Spreadability value: 13.33 g·cm/sec
20 Conclusion: The Moisturiser shows good spreadability as a spreadability value of
12-14 g·cm/sec is generally considered good for a topical cream. This indicates that
the moisturiser spreads easily, providing smooth application and good coverage on
the skin. This result further suggests that the cream formulation has a favourable
texture and is easy to apply, which enhances its consumer acceptability.
Viscosity (at 25°C) (Spindle
No. S-93, Speed: 0.5 RPM)
50,000 cp
13
Skin Irritancy Test:
A small amount (0.5 g) of the moisturiser was applied behind the ear of each
volunteer. The product was left on for 24 hours, and the skin was examined at 24,
48, and 72 hours for any signs of irritation. The results are depicted in Table 4
5 below.
Scoring system:
0: No reaction
1: Mild redness
2: Moderate redness or slight swelling
10 3: Severe redness, swelling, or itching
4: Extreme redness, blistering, or discomfort
Table 4: Evaluation of Skin Irritation volunteers
Sr No Volunteer Redness
(Erythema)
Swelling
(Edema)
Overall
Irritation Score
1 0 0 0 0
2 0 0 0 0
3 0 0 0 0
4 0 0 0 0
5 0 0 0 0
6 0 0 0 0
7 0 0 0 0
8 0 0 0 0
9 0 0 0 0
10 0 0 0 0
11 0 0 0 0
12 0 0 0 0
13 0 0 0 0
14 0 0 0 0
15 0 0 0 0
16 0 0 0 0
17 0 0 0 0
18 0 0 0 0
19 0 0 0 0
20
0 0 0 0
14
Overall, the Antioxidant moisturizer demonstrated excellent tolerability with no
irritancy, indicating that it is safe for use in the tested population.
Comedogenic and Skin Irritation Evaluation in Laboratory via Patch Test
5 Below are the laboratory testing report results:
15
The dermatology report during laboratory testing of the said herbal anti-oxidant
moisturizing cream indicates 0 score for comedogenic rating with no irritation
thereby confirming that the said 5 cream depicts no comedones or skin irritation.
Further, microbial analysis during laboratory testing confirms the anti-microbial
activity and thermal stability. , Claims:1) A herbal anti-oxidant moisturizing formulation comprising of;
- 4% each of cold compressed Grapeseed oil, cold compressed Rosehip
oil, cold compressed Jojoba oil and cold compressed Argan oil;
- 0.5% each of Liquorice Liquid Extract, 5 Papaya Liquid Extract and
Carrot seed Liquid Extract;
- 2% each of Candelilla wax, Shea butter and Glycerin;
- 1% each of Geogard ECT, Vitamin E and Cherry blossom Flavour;
- 9% Emulsifying wax;
10 - 0.02% Rose Pink Mica Powder and
- 64.48% (q.s. to make 100 gms) distilled water.
2) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, Grapeseed oil, Rosehip oil, Jojoba oil and Argan oil in the said
formulation are non-comedogenic oils that synergistically enhances
15 moisturizing, hydrating and antioxidant properties of the said formulation.
3) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the said formulation is a cream-based vegan formulation.
4) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the pH of the said herbal anti-oxidant moisturizing cream is in the
20 range of 5.5 - 7 with the preferred pH of 6.5.
5) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the viscosity of the said herbal anti-oxidant moisturizing cream is
in the range of 20000 - 100000 cps with the preferred viscosity of 50,000
cp.
17
6) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the dermatology report during laboratory testing of the said herbal
anti-oxidant moisturizing cream depicts 0 score for comedogenic rating with
no irritation thereby confirming that the said cream indicates no comedones
5 or skin irritation.
7) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the said herbal anti-oxidant moisturizing cream is thermally stable.
8) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the said herbal anti-oxidant moisturizing cream is suitable for wide
10 range of skin types including dry skin, oily skin, sensitive and acne-prone
skin.
9) The herbal anti-oxidant moisturizing formulation as claimed in claim 1
wherein, the said herbal anti-oxidant moisturizing cream hydrates, protects,
and rejuvenates the skin with no risk of clogged pores and irritation.
15 10) A method of preparation of herbal anti-oxidant moisturizing cream
comprising of;
a. adding Grapeseed oil, Rosehip oil, Jojoba oil, Argan oil, emulsifying
wax, candelilla wax and Shea Butter in a prescribed quantity in a
container and melting the same in the water bath at maintained
20 temperature of 70°-80°C under slow stirring to form oil phase;
b. adding distilled water and glycerin in the prescribed quantity in another
container and heating the same in the water bath at maintained
temperature of 70°-80°C under slow stirring to form aqueous phase;
c. filtration of oil phase in step a. through sieve no. 100 and adding the
25 same to aqueous phase;
d. mixing and homogenizing the mixture prepared in step c. up to 30 mins
until formation of cream;
18
e. continue mixing until the cream base is cooled to 40°-45°C;
f. adding Geogard ECT, Vitamin E, Cherry blossom Flavour, Liquorice
Liquid Extract, Papaya Liquid Extract and Carrot seed Liquid Extract
along with Rose Pink Mica Powder to the cream base in step g under
slow stirring initially 5 and continuous stirring later with homogenization
for 10 minutes.

Documents

NameDate
202421088467-FORM 18 [17-12-2024(online)].pdf17/12/2024
202421088467-COMPLETE SPECIFICATION [15-11-2024(online)].pdf15/11/2024
202421088467-DECLARATION OF INVENTORSHIP (FORM 5) [15-11-2024(online)].pdf15/11/2024
202421088467-FORM 1 [15-11-2024(online)].pdf15/11/2024
202421088467-FORM-26 [15-11-2024(online)].pdf15/11/2024
202421088467-FORM-9 [15-11-2024(online)].pdf15/11/2024

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