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ADVANCED METHOD FOR EXTRACTING NATURAL DYES FROM TEMPLE FLOWER WASTE USING INTEGRATED MULTI-EXTRACTION TECHNIQUES

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ADVANCED METHOD FOR EXTRACTING NATURAL DYES FROM TEMPLE FLOWER WASTE USING INTEGRATED MULTI-EXTRACTION TECHNIQUES

ORDINARY APPLICATION

Published

date

Filed on 4 November 2024

Abstract

The invention presents an innovative method for extracting natural dyes from temple flower waste, utilizing an integrated approach that combines enzymatic extraction, supercritical fluid extraction (SFE), and Magneto-Fluid Dynamic Extraction (MFDE). This multi-faceted technique enhances pigment yield and quality while minimizing environmental impact, providing a sustainable alternative to synthetic dyes. The process involves optimizing enzyme selection, extraction conditions, and the application of a magnetic field to improve efficiency. Additionally, the invention promotes the creation of dynamic artworks that respond to environmental stimuli, fostering cultural appreciation and community engagement. By transforming temple flower waste into valuable resources for artistic expression, this invention contributes to environmental conservation and the preservation of cultural heritage, offering new possibilities for eco-friendly art practices.

Patent Information

Application ID202411084066
Invention FieldCHEMICAL
Date of Application04/11/2024
Publication Number46/2024

Inventors

NameAddressCountryNationality
Ritik SharmaDepartment of Chemical Engineering, Chandigarh University, National Highway 05, Chandigarh-Ludhiana Highway, Mohali, Punjab -140413, IndiaIndiaIndia
Tripti SharmaDepartment of UIPS, Chandigarh University, National Highway 05, Chandigarh-Ludhiana Highway, Mohali, Punjab -140413, IndiaIndiaIndia

Applicants

NameAddressCountryNationality
Chandigarh UniversityChandigarh University National Highway 05, Chandigarh-Ludhiana Highway, Mohali, Punjab -140413, IndiaIndiaIndia

Specification

Description:The present invention relates to an advanced method for extracting natural dyes from temple flower waste, which is a high yield and quality extraction method minimizing environmental impact. The process is of great importance since temples generate much floral waste that remains unused and contributes to environmental degradation. This technique covers a systematic procedure from the collection of fresh temple flowers, preparation, and finally extraction in a series of innovative techniques. Different versions of this invention are so designed that the natural properties of the wastes generated from flowers are used in such a way that the dyes produced are not only rich and durable but also sustainable.
In the initial embodiment, the process begins by collecting and preparing flower waste with utmost care. Flowers are collected from temples; the flowers gathered are devoid of germs. The preparation stage involves removing non-floral wastes and then drying which does not spoil the virtue of the flowers. Drying is done in a well ventilated place without exposure to direct sunlight to avoid the oxidation that may oxidise further the natural pigments. It is this in depth preparation which provides a foundation that follows the extraction process afterward, allowing raw materials of optimal quality to be available for the extraction of dyes.
The core of the invention lies in the integration of three distinct extraction techniques: enzymatic extraction, supercritical fluid extraction (SFE), and Magneto-Fluid Dynamic Extraction (MFDE). The process of enzymatic extraction depends upon specific enzymes that break down certain parts of cell walls of plants, thus prompting the leakage of pigments. Optimum conditions of temperature and pH levels further enhances the efficiency of pigment discharge through this process. Post some enzymatic treatment, SFE is used, which extracts using supercritical CO2 as a solvent to further extract pigments from the textiles. Considering the unique solubility properties of supercritical fluids, this process leaves excellent-quality pigment extraction with minimal amounts of solvent in use.
The introduction of the novel Magneto-Fluid Dynamic Extraction (MFDE) technique marks a significant advancement in the extraction process. This embodiment utilizes a magnetic field to influence the fluid dynamics of the extraction medium, enhancing the penetration of solvents into plant tissues. By applying a magnetic field, the movement of solvent molecules is accelerated, resulting in improved extraction rates and higher pigment concentrations. The design of the extraction unit incorporates magnetic field generators, allowing for a seamless integration of this cutting-edge technique with conventional extraction methods. The combination of these extraction techniques not only increases dye yield but also provides a more environmentally friendly approach by reducing the need for harsh solvents.
The final concentration and stabilization of the extracted pigment solutions are carried out to increase the usability of the extracted pigment solutions in artistic applications. This is a concentration phase through evaporation techniques applied gently as well as through the stabilization of color by natural mordants, which fixes the color but also, when applied to any form of artistic medium, gives life durability. With these final pigments, use them in a range of applications as diverse as conventional painting and collage making to some new 3D printing techniques, thus opening new roads towards creativity while pursuing environmentally-friendly applications.
Key Aspects and Process of the Invention
1. Collection and Preparation of Flower Waste
The process begins with collecting temple flowers, which are basically natural pigments; hence utmost cleanliness is being observed in the collection to avoid contamination. Once the flowers have been collected, it is important that the flowers be carefully freed of floral debris such as leaves and stems. Then, flower petals were dried in a relatively ventilated area but shaded to still somewhat retain bright colors and chemical structure. It is this stage, the preparation stage that actually forms a prerequisite for a favorable pigment extraction in the following stages.
2. Enzymatic Extraction
The enzymatic extraction process employs specific enzymes tailored to break down the cell walls of the flower material. By optimizing parameters such as temperature and pH, this method enhances the release of pigments significantly. The use of enzymes is advantageous as it operates under mild conditions, minimizing the degradation of sensitive compounds and maximizing the yield of natural dyes. The extraction method ensures that a goodly amount of pigments, which means that there is being a richer color palette for application.
3. Supercritical Fluid Extraction (SFE)
The next process after the enzymatic treatment is a supercritical fluid extraction, which utilizes a supercritical CO2 as the extraction solvent. This technique takes advantage from the technique of supercritical fluids that permits efficient and selective extraction of pigments. The Supercritical Fluid Extraction (SFE) also obtains higher purity stages with lesser consumption of solvents. Thus, enzymatic extraction in combination with SFE forms a comprehensive extraction process and ensures natural dyes of fine quality with their respective vibrancy and stability.
In the integrated multi-extraction techniques, supercritical fluid extraction (SFE) employs supercritical CO2 at pressures ranging from 800 psi to 1200 psi. This specific pressure range is crucial as it significantly enhances the solubility of various pigments, improving the efficiency of the extraction process. Higher pressures facilitate better solvent penetration into the plant matrix, maximizing pigment yield and allowing for a broader spectrum of dye extraction. This technical advancement not only optimizes extraction tailored to the specific pigments in different temple flower species but also reduces the reliance on organic solvents, making the process more environmentally friendly. Combined with enzymatic extraction and Magneto-Fluid Dynamic Extraction (MFDE), the use of optimized SFE pressures results in faster extraction times and higher pigment concentrations, contributing to a more sustainable and effective method of producing natural dyes.
4. Magneto-Fluid Dynamic Extraction (MFDE)
The innovative Magneto-Fluid Dynamic Extraction (MFDE) method introduces a magnetic field into the extraction process, enhancing the dynamics of the fluid and improving solvent penetration into the plant tissue. The solvent molecules move faster, and consequently, the rate of extraction of the pigments increases highly. This provides a real-time extraction unit, custom designed by incorporating magnetic field generators, in which the extraction efficiency is being controlled. By reducing extraction times and pigment concentrations, MFDE, therefore contributes toward improving the extraction of dyes in a more sustainable fashion aligned with modern eco-friendly practices.
5. Concentration and Stabilization of Pigments
After the extraction processes, the resulting pigment solutions are concentrated through gentle evaporation methods that do not compromise the integrity of the pigments. At this point, concentration to build the viscosities necessary for artistic applications is critical. The presence of extracted colors with natural mordants ensures longevity and stabilizes the dyes for use on different substrates. This stabilizing process is particularly meaningful for art, as colorfastness is crucially important. The final pigments are then being employed through all of these different artistic media. This spectrum of pigments provides artists with a versatile and environmentally friendly coloring options.
The natural mordants selected from alum, iron, and tannin are employed to stabilize the extracted colors. These eco-friendly mordants enhance the binding of pigments to various artistic mediums, significantly improving lightfastness and wash fastness. This approach represents a technical advancement by replacing synthetic mordants with sustainable alternatives, aligning with the invention's goal of promoting environmentally friendly practices in art materials. By utilizing these natural mordants, the process not only reduces reliance on harmful chemicals but also supports the overall sustainability and cultural appreciation central to the use of temple flower waste in art.
6. Applications of Natural Dyes
The natural dyes extracted through this innovative method find a wide range of applications in the art world. Artists employ these dyes in traditional forms such as painting and collage-making, as well as in modern techniques like 3D printing, where bio-inks are being developed for intricate designs. The versatility of these natural dyes allows for creative exploration while adhering to sustainable practices. Additionally, the integration of these dyes into various artistic mediums fosters a deeper appreciation for environmental consciousness in the arts, highlighting the potential of waste materials as valuable resources.
The invention includes the innovative use of extracted dyes in artworks created using the extracted natural dyes can be constructed from materials selected from textiles, paper, and biodegradable plastics that are responsive to variations in light, temperature, or humidity. This introduces a dynamic element to artistic expression, allowing artworks to interact with their environment and change appearance based on external stimuli. This capability represents a significant advancement in art materials by merging traditional dyeing techniques with modern smart technology. By incorporating responsive dyes, artists create pieces that not only convey aesthetic value but also engage viewers through their changing characteristics. This responsiveness fosters a deeper connection between the artwork and the environment, enhancing the cultural significance of art derived from temple flower waste. Furthermore, it showcases the potential of natural dyes to meet contemporary artistic demands, bridging sustainability with innovation in creative practices.
By utilizing textiles, paper, and biodegradable plastics, the invention not only supports sustainable practices but also encourages the use of renewable resources. These materials align with principles of reducing waste and environmental impact, particularly through the repurposing of temple flower waste. The combination of natural dyes with these eco-friendly substrates enhances the artistic potential and durability of the works, ensuring that they remain vibrant and functional while contributing positively to the environment. This integration of materials fosters innovation in artistic expression, allowing for diverse applications in contemporary art practices.
7. Environmental and Cultural Benefits
This innovation impacts the environment much as it looks to reduce dependence on synthetic dyes while minimizing waste in its use of temple flower waste. Along with this change in the face of environmental challenges, the discovery encourages culture preservation. Through such a creative process of transforming religious offerings into art, the product honours culture and engages local people in more activities of sustainability. This dual focus on environmental conservation and cultural appreciation gives the overall value to the invention as putting it as a strong contribution toward both art and ecologically friendly practices.
According to one of the embodiment of the present invention, Figure 1 (100) detailed about the process of flower/floral waste collection (101), cleaning and drying of flowers (102), integrated multi-extraction techniques (103) that further comprises enzymatic extraction to enhance pigment release (104) and supercritical fluid extraction to extract pigments using supercritical CO2 (105), followed by magnetic fluid dynamic extraction (106), introducing magnetic field for the enhancement of fluid dynamics (107) and the final yielding of natural dyes (108).
In another embodiment of the present invention, Figure 2 (200) detailed about the process of concentration and stabilization of pigments (201) followed by gentle evaporation (202), stabilizing natural dyes (203) and finally the obtained concentrated pigmented solutions (204).
Furthermore, present invention offers a new process of extracting natural dyes from temple flower waste using an integrated multi-extraction approach. Here, it combines enzymatic extraction, supercritical fluid extraction, and innovative magneto-fluid dynamic extraction to improve the yield and quality of produced natural dyes while having minimal adverse impacts on the environment. The process not only solves problems caused by floral waste but also steps into sustainable and cultural respect in the act of the art.
The detailed descriptions of the embodiments highlight the systematic approach taken in the collection, preparation, and extraction of natural pigments, ensuring optimal quality throughout. The natural dyes produced through this is not just be an environmentally friendly alternative to synthetic dyes but also allow any application from paintings with newer technologies like 3D printing.
The environmental benefits of utilizing temple flower waste are significant, contributing to waste reduction and fostering a deeper engagement with cultural practices. By transforming what otherwise being discarded into valuable artistic resources, this invention honors local traditions while championing eco-friendly practices.
Therefore, this novel method and seek to protect it through this patent application, paving the way for further innovations in sustainable art materials and practices. The application is being favorably considered in the interest of promoting environmental sustainability and cultural heritage in the arts.
, Claims:1. A method for extracting natural dyes from temple flower waste, comprising:
collecting and preparing temple flower waste;
performing enzymatic extraction to enhance pigment release;
utilizing supercritical fluid extraction (SFE) to further extract pigments; and
applying Magneto-Fluid Dynamic Extraction (MFDE) to improve extraction efficiency.
2. The method of claim 1, wherein the enzymatic extraction process includes selecting specific enzymes that break down plant cell walls and optimizing conditions of temperature and pH.
3. The method of claim 1, wherein the supercritical fluid extraction employs supercritical CO2 at pressures ranging from 800 psi to 1200 psi.
4. The method of claim 1, further comprising stabilizing the extracted dyes by concentrating the pigment solutions through gentle evaporation and applying natural mordants.
5. The method of claim 4, wherein the natural mordants used are selected from alum, iron, and tannin.
6. The method of claim 1, wherein the collected flower waste is dried in a ventilated area away from direct sunlight before extraction.
7. The method of claim 1, wherein the extraction process reduces reliance on synthetic dyes and minimizes environmental impact through the use of temple flower waste.
8. A process for creating dynamic artworks using natural dyes extracted from temple flower waste, comprising:
integrating natural dyes that change color based on environmental stimuli;
utilizing the extracted dyes in artworks responsive to variations in light, temperature, or humidity.
9. The process of claim 8, wherein the artworks are constructed from materials selected from the group consisting of textiles, paper, and biodegradable plastics.
10. The process of claim 8, further comprising engaging local communities in the creation of artworks to foster cultural appreciation and heritage.

Documents

NameDate
202411084066-COMPLETE SPECIFICATION [04-11-2024(online)].pdf04/11/2024
202411084066-DECLARATION OF INVENTORSHIP (FORM 5) [04-11-2024(online)].pdf04/11/2024
202411084066-DRAWINGS [04-11-2024(online)].pdf04/11/2024
202411084066-EDUCATIONAL INSTITUTION(S) [04-11-2024(online)].pdf04/11/2024
202411084066-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [04-11-2024(online)].pdf04/11/2024
202411084066-FIGURE OF ABSTRACT [04-11-2024(online)].pdf04/11/2024
202411084066-FORM 1 [04-11-2024(online)].pdf04/11/2024
202411084066-FORM FOR SMALL ENTITY(FORM-28) [04-11-2024(online)].pdf04/11/2024
202411084066-FORM-9 [04-11-2024(online)].pdf04/11/2024
202411084066-POWER OF AUTHORITY [04-11-2024(online)].pdf04/11/2024
202411084066-PROOF OF RIGHT [04-11-2024(online)].pdf04/11/2024
202411084066-REQUEST FOR EARLY PUBLICATION(FORM-9) [04-11-2024(online)].pdf04/11/2024

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